中國醫藥大學機構典藏 China Medical University Repository, Taiwan:Item 310903500/30630
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    题名: Efficacy of pelvic floor rehabilitation for treatment of genuine stress incontinence
    作者: Chen, HY;Chang, WC;Lin, WC;Yeh, LS;Hsu, TY;Tsai, HD;Yang, KY
    贡献者: 醫學院醫學系寄生蟲學科;China Med Coll Hosp, Dept Obstet & Gynecol, Taichung, Taiwan;China Med Coll Hosp, Urodynam Unit, Taichung, Taiwan
    日期: 1999
    上传时间: 2010-09-24 14:58:57 (UTC+8)
    出版者: EXCERPTA MEDICA ASIA LTD
    摘要: Under mild conditions, reactions of (CO)(5)M=C[N(R)CH2](2) [M = W, Mo, Cr; R = Et, allyl, benzyl, 4-pentenyl] with (PhCN)(2)PdCl2, (PhCN)(2)PtCl2, [(CO)(2)RhCl](2), (Me2S)AuCl, [(CH3CN)(4)Cu]BF4, and AgBF4 provide the corresponding diaminocarbene complexes via carbene ligand transfer. The resulting Pd(II), Pt(II), Rh(I), and Au(I) carbene complexes are stable and were isolated. The Cu(I) and Ag(I) complexes readily undergo acid-induced M=C cleavage to yield the imidazolidin-2-ylidinium salts. The carbene-transfer reactions were studied for two phosphine donors: (CO)(m)(L)W=C[N(R)CH2](2) CR = Et, benzyl; L = PPh3, m = 4; L = dppe, m = 3). The X-ray crystal structures of (CO)(5)W=C[N(CH2C6H5)CH2](2) (1c), cis-(CO)(4)(PPh3)W=C[N(CH2C6H5)CH2](2) (5b), fac-(CO)(3)(dppe)W=C[N(CH2C6H5)CH2](2) (6b), Cl-2(CO)Pt=C[N(CH2C6H5)CH2](2) (9c), and cis-Cl2Pt{=C[N(CH2C6H5)CH2](2)}(2) (11b) are reported.
    關聯: JOURNAL OF THE FORMOSAN MEDICAL ASSOCIATION 98(4):271-276
    显示于类别:[醫學系] 期刊論文

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