摘要: | 實驗目的;牙科複合樹脂常用於美觀區域的復型。本研究之目的在比較牙科充填用奈米複合樹脂及傳統複合。
實驗步驟;實驗材料包括5種牙科奈米複合樹脂:(1) Gradia○R Anterior (Voco公司)、(2) Grandia○R Posterior (Voco公司)、(3) Mono○R(Dentsply公司)、(4) FiltekTM Z350○R (3M公司)、(5) Esthet○R (Dentsply公司),以及3種牙科傳統複合樹脂:(1) Primedent○R (Prime Dental Manufacturing公司)、(2) Spectrum○R (3M公司)、(3) FiltekTM Z100○R (3M公司) 。經過不同溶液(1)蒸餾水(2)酒精(3)醋酸(4)醬油(5)紅茶各浸泡15天後,分別測試其機械性質:(1)吸水量變化(2)顏色變化(3)表面粗度(4)表面硬度,每次測試皆重複5次,以two way ANOVA及paired t test 分析比較浸泡前後差異、奈米與傳統複合樹脂間差異(p value<0.05)。
實驗假設;預期奈米材料有較好的性質表現。
實驗結果;
(1)吸水量變化:奈米樹脂吸水量並非一定比傳統樹脂少,醋酸對Primedent○R,Spectrum○R,Gradia○R Anterior,Grandia○R Posterior, FiltekTM Z350○R, Esthet○R 吸水量有顯著影響(p<0.05)
(2)顏色變化:奈米樹脂色差值並非一定比傳統樹脂少,醋酸對Primedent○R,Spectrum○R,Grandia○R Posterior,Mono○RFiltekTM Z350○R, Esthet○R 色差值有顯著影響(p<0.05)。
(3)表面粗度;奈米樹脂浸泡後表面粗度並非一定比傳統樹脂小,醋酸對所有材料Primedent○R, Spectrum○R,FiltekTM Z100○R,Gradia○R Anterior,Grandia○R Posterior,Mono○RFiltekTM Z350○R, Esthet○R 表面粗度有顯著影響(p<0.05)。
(4)表面硬度;浸泡後所有材料表面硬度皆有下降(p<0.05)。 Primedent○R, Spectrum○R,FiltekTM Z100○R,Gradia○R Anterior,Grandia○R Posterior,FiltekTM Z350○R, Esthet○R 在醋酸中表面硬度最低。 (p<0.05)。
結論; 本實驗無法證實奈米樹脂的蓮花效應、自淨作用、表面粗度穩定性、表面硬度穩定性如同外界聲稱之好。本實驗發現醋酸對大部分的材料性質有明顯的影響。樹脂材料特性並不能用傳統樹脂與奈米樹脂的分類一概而論,材料特性仍須分別探討。
Purpose;Dental composite resin is commonly used for restoration in esthetic area. The purpose of this study is to compare mechanical properties of dental nanocomposite and conventional composite.
Materials and Method;Five brands of nanocomposite were selected to be investigated, (1) Gradia○R Anterior (Voco, Germany), (2) Grandia○R Posterior (Voco, Germany), (3) Mono○R(Dentsply, Germany), (4) FiltekTM Z350○R (3M, USA), and (5) Esthet○R (Dentsply, USA). Three brands of conventional composite were selected to be researched, (1) Primedent○R (Prime Dental Manufacturing, USA), (2) Spectrum○R (3M, USA), (3) FiltekTM Z100○R (3M, USA) . Every material were soaked in five liquids ; each for 15 days, (1)diluted water, (2)alcohol, (3)acetic acid, (4)black tea, (5)soy bean sauce. Before and after 15 days immersion each specimen was tested and repeated 5 times. Mechanical properties such as (1)water immersion, (2)color change, (3)surface roughness, and (4)surface hardness were recorded and statistically analyzed with paired t test and two-way ANOVA. A significance level of p-value < 0.05 was chosen.
Hypothesis: All nanocomposites have better mechanical properties.
Results: (1)Water immersion: Not all nanocomposites have less water immersion than conventional composites. Acetic acid has significant effect at water immersion of Primedent○R, Spectrum○R, Gradia○R Anterior, Grandia○R Posterior, FiltekTM Z350○R, and Esthet○R (p<0.05)
(2)Color change: Not all nanocomposites have less color change than conventional composites. Acetic acid has significant effect at color change of Primedent○R, Spectrum○R, Grandia○R Posterior, Mono○RFiltekTM Z350○R, Esthet○R(p<0.05)。
(3)Surface roughness: After 15 days immersion, not all nanocomposites have lower surface roughness than conventional composites. Acetic acid has significant effect at surface roughness of Primedent○R, Spectrum○R, FiltekTM Z100○R, Gradia○R Anterior, Grandia○R Posterior, Mono○RFiltekTM Z350○R, and Esthet○R(p<0.05)。
(4)Surface hardness: After 15 days immersion, all materials have lower surface roughness than before immersion(p<0.05). Acetic acid has significant effect at surface hardness of Primedent○R, Spectrum○R, FiltekTM Z100○R, Gradia○R Anterior, Grandia○R Posterior, FiltekTM Z350○Rand Esthet○R (p<0.05). |