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    題名: Langerhans cell histiocytosis of the skull complicated with an epidural hematoma
    作者: Chen, HC;Shen, WC;Chou, DY;Chiang, IP
    貢獻者: 附設醫院放射線部;China Med Coll Hosp, Dept Radiol, Taichung 407, Taiwan;China Med Coll Hosp, Dept Neurosurg, Taichung 407, Taiwan;China Med Coll Hosp, Dept Pathol, Taichung 407, Taiwan
    日期: 2002
    上傳時間: 2010-09-24 14:31:04 (UTC+8)
    出版者: AMER SOC NEURORADIOLOGY
    摘要: A solid-phase microextraction (SPME) device was used as a time-weighted average sampler for n-valeraldehyde. The SPME device was first modified to improve the wearer's acceptance as a passive sampler. Then a poly (dimethyl siloxane)divinylbenzene fiber was used and O-2,3,4,5,6-(pentafluorobenzyl)hydroxylamine hydrochloride (PFBHA) was loaded onto the fiber. Vapors of known concentrations around the threshold limit values time-weighted average of n-valeraldehyde and specific relative humidities (RHs) were generated by syringe pumps in a dynamic generation system. n-Valeraldehyde vapors in gas bags were also generated. An exposure chamber was designed to allow measurement of face velocities, temperatures, exposing vapor concentrations, and RHs. Gas chromatography with flame ionization detection was used for sample analysis. The appropriate adsorption time for SPME coating PFBHA was determined to be 2 min and the desorption time for oxime formed after sampling was optimized to be 2 min. The experimental sampling constant was found to be (3.86+/-0.13)(.)10(-2) cm(3)/min and face velocity was not expect to have effect on the sampler. (C) 2002 Elsevier Science B V All rights reserved.
    關聯: AMERICAN JOURNAL OF NEURORADIOLOGY 23(3):493-495
    顯示於類別:[台中附設醫院] 期刊論文

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